Reference of 1217-45-4,Some common heterocyclic compound, 1217-45-4, name is 9,10-Anthracenedicarbonitrile, molecular formula is C16H8N2, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
EXAMPLE 99 STR107 (+-)-Cis-3,4,9,9a-tetrahydroindeno[2,1-c]thiopyran-4a(1H)-amine To a solution of the benzylamine (1.0 g, 3.4 mmol) from Example 98 in acetonitrile/water (7:3) is added 9,10-dicyanoanthracene. The reaction is irradiated as described in Tetrahedron Letters 29, 4157 (1988). The reaction yields the primary amine which is converted to the title compound.
The synthetic route of 1217-45-4 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Bigge; Christopher F.; Hays; Sheryl J.; Johnson; Graham; Novak; Perry M.; Ortwine; Daniel F.; US5071853; (1991); A;,
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts