Category: 10365-94-3

Reference of 10365-94-3, A common heterocyclic compound, 10365-94-3, name is 1,3,5-Benzenetricarbonitrile, molecular formula is C9H3N3, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.

REFERENCE EXAMPLE 1 In an autoclave of a 300-ml content fitted with an electromagnetic agitator was placed for tight sealing a mixture of 15 g of 1,3,5-tricyanobenzene (MTN), 15 g of Raney-nickel.chromium catalyst prepared according to the conventional method (atomic ratio of Ni_Cr=49:1), 27 ml of methanol, 63 ml of m-xylene and 0.18 g of caustic soda, and hydrogen was charged at an initial pressure of 100 kg/cm2 G to conduct the reaction at 100 C., resulting in the absorption of 0.59 mole of hydrogen over a 35-minute period. The catalyst was filtrated out and the solvent was distilled off, followed by conducting vacuum distillation, thus resulting in 12.8 g of 1,3,5-tris(aminomethyl)benzene (MTA).

The synthetic route of 10365-94-3 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; Takeda Chemical Industries, Ltd.; US4338256; (1982); A;,
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 10365-94-3, name is 1,3,5-Benzenetricarbonitrile, This compound has unique chemical properties. The synthetic route is as follows., Quality Control of 1,3,5-Benzenetricarbonitrile

(3) 100 g of 1,3,5-benzotrinitrile and 3 g of Raney-Ni, 400 mL of ethanol are added to a 1 L hydrogenation reactor, and H2 is continuously charged, so that the pressure of the system is always maintained at 8 MPa during the reaction. After the reaction was performed at a reaction temperature of 110 C. for 1.5 h, the temperature was lowered. When the temperature in the reaction vessel was lowered to room temperature, the gas was purged, and 1,3,5-benzenetrimethylamine (having a purity of 99% or more) was obtained by filtration and recrystallization. The yield was 88% by weight.

According to the analysis of related databases, 10365-94-3, the application of this compound in the production field has become more and more popular.

Reference:
Patent; Sinopec Yangzi Petrochemical Co., Ltd.; Sinopec Corporation; Sun Hailong; Li Na; Gao Yilong; Wei Yanyu; Chen Xinhua; Miao Jun; Kan Lin; Bai Jiye; Chen Shaohui; Yang Aiwu; Xu Yuexing; (30 pag.)CN105001032; (2018); B;,
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts

Application of 10365-94-3, These common heterocyclic compound, 10365-94-3, name is 1,3,5-Benzenetricarbonitrile, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.

Example 20:; Production of D-141:; D-141 was produced according to the following scheme:Production of D-141A:; 100 ml of methanol was added to 11.5 g of 1,3,5- tricyanobenzene produced in an ordinary manner, and then 26.0 ml of 50 % hydroxylamine solution was added to it, and stirred at 6O0C for 3 hours. After cooled, water was added to the reaction liquid, and the deposited crystal was taken out through filtration and dried to obtain 8.0 g of a crystal of D-141A.

Statistics shows that 1,3,5-Benzenetricarbonitrile is playing an increasingly important role. we look forward to future research findings about 10365-94-3.