Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 6136-93-2, name is 2,2-Diethoxyacetonitrile, This compound has unique chemical properties. The synthetic route is as follows., SDS of cas: 6136-93-2
In a round bottom flask, ammonium sulfide (44 wt% in H2O, 17.4 mL, 112 mmol) was added to a solution of diethoxyacetonitrile (6) (11.1 mL, 80.0 mmol) in MeOH (770 mL). The mixture was stirred at room temperature for 22 h. The solvent was evaporated under reduced pressure to afford thioamide 7 (13.0 g, quantitative yield) as a pale yellow solid. TLC: Rf 0.63 (1:1 hexane/EtOAc). Mp: 87.5-89.5 C (lit.81-82 C). IR (KBr, film): 3370,3182, 2975, 1124, 1064 cm1. 1H NMR (400 MHz, CDCl3): d 7.86(br s, 1H), 7.52 (br s, 1H), 5.05 (s, 1H), 3.74 (dq, 2H, J = 9.6,7.2 Hz), 3.64 (dq, 2H, J = 9.6, 7.2 Hz), 1.26 (t, 6H, J = 7.2 Hz).13C NMR (100 MHz, CDCl3): d 202.2, 103.2, 63.1, 15.2. HRMS (ESI)m/z calculated for C6H13NO2S 163.0667, found 163.0664.
According to the analysis of related databases, 6136-93-2, the application of this compound in the production field has become more and more popular.
Reference:
Article; Park, Yunjeong; Bae, Song Yi; Hah, Jung-Mi; Lee, Sang Kook; Ryu, Jae-Sang; Bioorganic and Medicinal Chemistry; vol. 23; 21; (2015); p. 6827 – 6843;,
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