Name: Bis(acetylacetonato)dioxomolybdenum(VI). The reaction of aromatic heterocyclic molecules with protons is called protonation. Aromatic heterocycles are more basic than benzene due to the participation of heteroatoms. Compound: Bis(acetylacetonato)dioxomolybdenum(VI), is researched, Molecular C10H14MoO6, CAS is 17524-05-9, about Styrene selective oxidation to benzaldehyde catalyzed by acylhydrazone Mo complexes: Reaction parameter effects and kinetics. Author is Yang, Shuang; Li, Gong; Yang, Yujie; Zhu, Mengdi; Fu, Yuejiao; Xing, Na; Shi, Lei.
Three acylhydrazone molybdenum complexes were synthesized for the first time: [MoO2L1(EtOH)] (1), [MoO2L2(EtOH)] (2), [MoO2L3(EtOH)] (3), [H2L1 = 4-bromo- N’-(3,5-dichloro-2-hydroxybenzylidene)benzohydrazide, H2L2 = N’-(3,5-dichloro-2-hydr- oxybenzylidene)-3-hydroxy-4-methoxybenzohydrazide, H2L3 = N’-(3,5-dichloro-2-hydro- xybenzylidene)-4-trifluoromethylbenzohydrazide]. They were characterized by FTIR, UV-visible, 1H NMR and thermogravimetric method. Their crystal structures were determined by single crystal x-ray diffraction. The Mo atoms in the complexes were in octahedral coordination, with the equatorial plane defined by the phenolate O, imino N and enalate O atoms of the hydrazone ligands and one oxo group, with the axial positions occupied by one oxo group and one ethanol O atom. The catalytic properties of the three complexes for styrene oxidation were studied.
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