Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 4110-35-4, name is 3,5-Dinitrobenzonitrile, A new synthetic method of this compound is introduced below., Formula: C7H3N3O4
General procedure: (Caution HMPA is not a friendly solvent). A solution of 0.5 g of a starting substrate in 15 ml of HMPA was kept at 155-160 C until the reactant was consumed (TLC; eluent, CHCl3). The reaction mass was cooled and poured into 150 ml of ice water. The precipitate was filtered off, washed with water and dried. The crude product was dissolved in chloroform, and the solution was filtered through a silica gel bed. The filtrate was evaporated, and the residue was crystallized from methanol.
The synthetic route of 4110-35-4 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Dutov, Mikhail D.; Serushkina, Olga V.; Mendeleev Communications; vol. 23; 3; (2013); p. 174 – 175;,
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts