Synthetic Route of 868-54-2, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 868-54-2, name is 2-Aminoprop-1-ene-1,1,3-tricarbonitrile belongs to nitriles-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
General procedure: A 10% aqueoussolution of KOH (11.20 ml, 20 mmol) and phenacyl bromide2-d (20 mmol) were added consecutively to a stirredsolution of malononitrile dimer 1 (1.32 g, 10 mmol) in DMF(20 ml). The mixture was stirred for 2 h at 20C and dilutedwith an equal volume of H2O. The formed precipitate wasfiltered off, washed with H2O, EtOH, and hexane.
The synthetic route of 2-Aminoprop-1-ene-1,1,3-tricarbonitrile has been constantly updated, and we look forward to future research findings.
Reference:
Article; Dyachenko, Vladimir D.; Toropov, Alexey N.; Rusanov, Eduard B.; Chemistry of Heterocyclic Compounds; vol. 51; 1; (2015); p. 31 – 33; Khim. Geterotsikl. Soedin.; vol. 51; 1; (2015); p. 31 – 33,3;,
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts