Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 3695-84-9, name is Methyl 2-cyano-3-phenylacrylate, This compound has unique chemical properties. The synthetic route is as follows., COA of Formula: C11H9NO2
General procedure: A mixture of pyrazoline-5-one 1 (5 mmol), activated olefin 2 (5 mmol) and sodium bromide (0.31 g, 3 mmol) in methanol (20 mL) was electrolyzed in undivided cellequipped with a magnetic stirrer, a graphite anode and an iron cathode at 20 C under a constant current density of 100 mA cm-2 (I = 500 mA, electrodes square5 cm2) until the quantity of electricity 2.5 Fmol-1 of charge was passed. After the electrolysis was finished, spirocyclopropylpyrazolone 3 was filtered out and dried under reduced pressure. An additional amount of spirocyclopropylpyrazolone was isolated as follows. The reaction mixture was concentrated to 5 mL and cooled to -10 C overnight and filtered.
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 3695-84-9.
Reference:
Article; Elinson, Michail N.; Dorofeeva, Evgeniya O.; Vereshchagin, Anatoly N.; Korshunov, Alexander D.; Egorov, Mikhail P.; Research on Chemical Intermediates; vol. 42; 3; (2016); p. 2191 – 2200;,
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