69395-13-7, name is 4-(2-Hydroxyethyl)benzonitrile, belongs to nitriles-buliding-blocks compound, is considered to be a conventional heterocyclic compound, which is widely used in drug synthesis. The chemical synthesis route is as follows. HPLC of Formula: C9H9NO
Reference Example 2 2- [4-(4,5-Dihydro-lH-imidazol-2-yl)-phenyn -ethylamine dihvdrochloride a) 4-F2-C1 ,3-Dioxo-l ,3-dihydro-isoindol-2-ylVethyl1-benzonitrileUnder argon, a solution of 4-(2-hydroxy-ethyl)-benzonitrile [HeIv. CMm. Acta 64 (1981) 1688-1703] (4.49 g, 30.5 mmol), phthalimide (4.94 g, 33.55 mmol), triphenylphosphine (8.8 g, 33.55 mmol) and dimethyl formamide (100 mL) was stirred at 0 C for 20 minutes, then diethyl azodicarboxylate (7.59 mL, 48.8 mmol) was added dropwise at 0 0C. The so obtained reaction mixture was stirred at room temperature overnight, then poured into ice-water (740 mL). The precipitated product was filtered off, washed with water and dried. The crude product was recrystallized from 2-propanol to yield 7.83 g (93 %) of the title compound as a yellow solid.
The synthetic route of 69395-13-7 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; RICHTER GEDEON VEGYESZETI GYAR RT.; WO2007/72092; (2007); A2;,
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts