Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 97165-77-0, name is 3,5-Dibromobenzonitrile, This compound has unique chemical properties. The synthetic route is as follows., HPLC of Formula: C7H3Br2N
Compound II – 2 (2.61 g, 10 mmol), compound III (2.06 g, 10 mmol), Pd (OAc)2(0.22 G, 1 mmol), BINAP (2, 2 ‘- bi-phenyl diphenylphosphino – 1, 1’ – binaphthyl, 0.62 g, 1 mmol) and t – BuOK (2.24 g, 20 mmol) is added to the 50 ml dry 1, 2 – dimethoxy ethane (DME), the reaction mixture is stirred under a nitrogen atmosphere overnight, detected in the TLC reaction is completed.The reaction mixture carefully dumped into 200 ml ice water, stirring, for 50 ml ¡Á 3 CH2Cl2Extraction, the combined extraction phase, for sequentially 1% dilute hydrochloric acid and salt is washed with water, dried with anhydrous sodium sulfate. Oil filtration to remove the drying agent, the filtrate on a rotary evaporator to dryness, the residue using silica gel column chromatography purification, to obtain compound IV – 2
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 97165-77-0.
Reference:
Patent; Guangdong Sai Bo Technology Co., Ltd.; Guo Huijun; (8 pag.)CN107903271; (2018); A;,
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts