HPLC of Formula: 17524-05-9. Aromatic heterocyclic compounds can also be classified according to the number of heteroatoms contained in the heterocycle: single heteroatom, two heteroatoms, three heteroatoms and four heteroatoms. Compound: Bis(acetylacetonato)dioxomolybdenum(VI), is researched, Molecular C10H14MoO6, CAS is 17524-05-9, about Crystal structures and supramolecular architectures of ONO donor hydrazone and solvent exchangeable dioxidomolybdenum(VI) complexes derived from 3,5-diiodosalicyaldehyde-4-methoxybenzoylhydrazone: Hirshfeld surface analysis and interaction energy calculations. Author is Kuriakose, Daly; Kurup, M. R. Prathapachandra.
A tridentate ONO donor aroylhydrazone, 3,5-diiodosalicyaldehyde-4-methoxybenzoylhydrazone (H2DSMB), and two of its cis-MoO2 complexes, [MoO2(DSMB)(H2O)](DMF)2 (1) and [MoO2(DSMB)(py)] (2), have been synthesized and characterized by different physico-chem. methods. The mol. structures were determined by single crystal x-ray diffraction studies. The aroylhydrazone H2DSMB crystallizes in a monoclinic space group with two identical mols. in the asym. unit. The complex [MoO2(DSMB)(H2O)](DMF)2 (1) crystallizes in a triclinic space group whereas the other complex, [MoO2(DSMB)(py)] (2), crystallizes in an orthorhombic crystal system. The distorted octahedral geometry around the Mo(VI) central atom is satisfied by the di-deprotonated dianionic hydrazone moiety and two oxido oxygen atoms, the sixth labile coordination site being occupied by oxygen/nitrogen atoms from solvent mols. The importance of van der Waals interactions in the formation of the elementary structure obtained from the single crystal x-ray diffraction was authenticated by Hirshfeld surface anal. The individual types of intermol. contacts and their impact on the crystal packing was investigated by the anal. of the Hirshfeld surfaces and the signatures on the two-dimensional fingerprint plots. Interaction energy calculations reveal that the dispersion energy framework is dominant over other energy frameworks. The thermal behavior and the nature of the water mol. in the complex [MoO2(DSMB)(H2O)](DMF)2 (1) is discussed. Furthermore, in vitro cytotoxicity studies of the synthesized aroylhydrazone and its Mo(VI) complexes against the lymphoma ascites cell line are also included.
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Reference:
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts