Discovery of C11H11NO2

According to the analysis of related databases, 1528-41-2, the application of this compound in the production field has become more and more popular.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 1528-41-2, name is Ethyl 2-(4-cyanophenyl)acetate, This compound has unique chemical properties. The synthetic route is as follows., HPLC of Formula: C11H11NO2

EXAMPLE 4 4-(2-Butoxy-5-chlorobenzamidomethyl)-phenylacetic acid 11.5 g Ethyl 4-aminomethylphenylacetate hydrochloride (m.p. 172 C.; prepared by the catalytic hydrogenation of ethyl 4-cyanophenylacetate) are suspended in 200 ml toluene. After the addition of 13.9 ml triethylamine, there is added dropwise, while cooling, a solution of 12.4 g 2-butoxy-5-chlorobenzoyl chloride in 10 ml toluene. The reaction mixture is subsequently heated under reflux for 2 hours, while stirring. After cooling, the toluene phase is treated successively with dilute hydrochloric acid, aqueous sodium bicarbonate solution and water and then evaporated. The evaporation residue is heated on a steambath with 2 N aqueous sodium hydroxide solution and the solution then filtered. The filtrate is acidified with dilute hydrochloric acid. The precipitated 4-(2-butoxy-5-chlorobenzamidomethyl)-phenylacetic acid is reprecipitated via its sodium salt and recrystallized from ethanol. The yield is 3.9 g (20% of theory); m.p. 198 C.

According to the analysis of related databases, 1528-41-2, the application of this compound in the production field has become more and more popular.

Reference:
Patent; Boehringer-Mannheim GmbH; US4207341; (1980); A;,
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts