Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 3032-92-6, name is 4-Ethynylbenzonitrile, This compound has unique chemical properties. The synthetic route is as follows., HPLC of Formula: C9H5N
Sequentially adding a catalyst in the reaction bottle (14.0 mg, 0.025 millimole, 5mol %), cesium carbonate (32.6 mg, 1.0 mmol), 4-ethynyl phenyl nitrile (63.6 mg, 0.5 mmol),N,N-dimethylformamide(3 ml), into the carbon dioxide, in the 50 C, reaction under normal pressure 16 hours. Reaction cooling to room temperature, diluted with water, acidified with hydrochloric acid, diethyl ether extraction, washing with saturated sodium chloride for ether level, dry anhydrous sodium sulfate, obtained product is vacuum to remove the solvent, the yield is 93%
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 3032-92-6.
Reference:
Patent; Suzhou University; Sun, Hongmei; Zhu, Fan; Lu, Bing; (10 pag.)CN105585473; (2016); A;,
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts