Adding a certain compound to certain chemical reactions, such as: 97165-77-0, name is 3,5-Dibromobenzonitrile, belongs to nitriles-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 97165-77-0, name: 3,5-Dibromobenzonitrile
15.0 g (52.2 mmol) of (9-phenyl-9H-carbazol-3-yl)boronic acid, 27.3 g (104 mmol) of 3,5-dibromobenzonitrile, 3.02 g (2.61 mmol) of tetrakistriphenylphosphine palladium(0) (Pd(PPh3)4), and 18.1 g (131 mmol) of potassium carbonate were added to a solution of 120 ml of THF and 60 ml of water and mixed. The mixed solution was then stirred under reflux. After completion of the reaction, the resulting reaction solution was cooled to room temperature, and an extraction process was performed thereon to remove an aqueous solution layer therefrom. The obtained residue was filtered through silica gel under reduced pressure, and the filtrate was concentrated under reduced pressure. The resulting residue was then separated by silica gel column chromatography, thereby providing 11.9 g (yield: 54%) of a desired compound, Intermediate (R). LC-Mass (cald: 422.04 g/mol, found: M+1=423 g/mol).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 3,5-Dibromobenzonitrile, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; SAMSUNG ELECTRONICS CO., LTD.; Samsung SDI Co., Ltd.; JUNG, Yongsik; HUH, Dalho; SON, Jhunmo; KWON, Eunsuk; KIM, Sangmo; LEE, Saeyoun; JEON, Soonok; CHUNG, Yeonsook; KIM, Jongsoo; IHN, Sooghang; (219 pag.)US2017/369439; (2017); A1;,
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts