Adding a certain compound to certain chemical reactions, such as: 76469-88-0, name is Methyl 4-(cyanomethyl)benzoate, belongs to nitriles-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 76469-88-0, SDS of cas: 76469-88-0
A solution of methyl 4- (cyanomethyl) benzoate 24, (2.0 g, 11.4 mmol) in 6M Sodium hydroxide (15 mi) and methanol (15 mL) was heated at 90 C. overnight. After concentrating the reaction mixture, the aqueous layer was washed with dichloromethane (30 mL chi 2), then acidified to pH~3 with 12 HC1. The aqueous solution was extracted with ethyl acetate (20 ml 2). Organics was combined, dried over Na2S< and evaporated in vacuo to give titled compound. (1.45 mg, 70%). [M+H]* = 181.4 (APCI+) .
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Reference:
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts