In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 619-72-7 as follows. Recommanded Product: 4-Nitrobenzonitrile
General procedure: Photocatalytic reactions were carried out in a round bottom Pyrex flask and irradiated using four high power blue light LEDs 3W lamp or by solar light under magnetic stirring at room temperature. Reaction conditions with solar light: the aromatic nitro compounds (0.05mmol) and anhydride (0.052mmol) were carried out in the presence of TiO2-P25 (0.03g) in EtOH (10mL) and irradiated under sunlight for 1-4 h. Reaction conditions with blue LED irradiation: aromatic nitro compounds (0.002mmol) and anhydride (0.0025mmol) were carried out in the presence of TiO2-P25 (0.08g) in EtOH (4mL), and irradiated by four high power blue light LEDs 3W lamp for 30 h. While stirring, the mixture became heterogeneous as the reaction progressed. The product yields were determined by gas chromatography monitoring. The structure of products were confirmed by NMR (see ESI1).
According to the analysis of related databases, 619-72-7, the application of this compound in the production field has become more and more popular.
Reference:
Article; Zand, Zahra; Kazemi, Foad; Partovi, Adel; Journal of Photochemistry and Photobiology B: Biology; vol. 152; (2015); p. 58 – 62;,
Nitrile – Wikipedia,
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