Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 613-46-7, name is 2-Naphthonitrile, A new synthetic method of this compound is introduced below., Safety of 2-Naphthonitrile
General procedure: Catalyst 1 (10 mol%) and HBpin (0.44 mmol) were added to aSchlenk flask inside the glove box, followed by the addition oforganic nitriles (0.2 mmol). The reaction mixture was heatedcontinuously at 65 C under neat condition or under toluene for astipulated time, as mentioned in Table 2. Toluene was then added,and the reaction mixture was filtered through a short plug of Celiteand evaporated under reduced pressure to obtain a solid residue.The diboryl amines are moisture- and air-sensitive, and henceexperimental procedures were conducted and NMR samples wereprepared inside the glove box. All products were characterizedusing multi-nuclear NMR spectroscopy, and details are given in thesupporting information.
The synthetic route of 613-46-7 has been constantly updated, and we look forward to future research findings.