In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 1194-65-6, name is 2,6-Dichlorobenzonitrile belongs to nitriles-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. category: nitriles-buliding-blocks
In a 500 ml reaction flask, 51.6 g (0.3 mol) of 2,6-dichlorobenzonitrile, 41.6 g of water, and 0.6 g of a 30% sodium hydroxide solution were added.The temperature was raised to 35 C, and 55.65 g (0.45 mol) of 27.5% hydrogen peroxide was added dropwise.After 5 hours, the addition is completed.After the completion of the dropwise addition, the sample was controlled, and 2,6-dichlorobenzonitrile was ?0.5% qualified. Filtered, the filter cake was rinsed with 83.2 g of water.The wet product is dried to obtain 2,6-dichlorobenzamide 55g.The purity was >99.0%, and the yield was 97%.
The synthetic route of 1194-65-6 has been constantly updated, and we look forward to future research findings.