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Highly Productive alpha-Alkylation of Ketones with Alcohols Mediated by an Ir-Oxalamidato/Solid Base Catalyst System
An Ir-oxalamidato complex in combination with a solid base (e.g., magnesium aluminometasilicate/Ca(OH)(2)) significantly improved the catalyst productivity in alpha-alkylation of methyl ketones with primary alcohols. Optimization through systematic variation of the oxalamidato ligand led to a practical turnover number (TON) of 10 000-40 000.
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