Analyzing the synthesis route of 236750-65-5

The synthetic route of 236750-65-5 has been constantly updated, and we look forward to future research findings.

Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 236750-65-5, name is 4,5-Bis(2-methoxyethoxy)-2-nitrobenzonitrile, A new synthetic method of this compound is introduced below., Formula: C13H16N2O6

(d) 2-amino-4, 5-bis (2-methoxyethoxy) benzonitrile:; To 4,5-bis (2-methoxyethoxy)-2-nitrobenzonitrile(10 g) was added acetic acid (75ml) and water(75ml), stirred the reaction mass for about 10 min, added Iron powder (7g) in portions over a period of 2hrs, Stirred the reaction mixture for about Vz hr at 300C adjusted PH of the reaction mass to 7. Extracted the material into ethylacetate, the organic layer was dried over sodium sulfate and concentrated to yield crystalline yellow solid. Which was further recrystallized from methanol (6g) mp 74-77 0C1HNMR (CDCI3): delta 3.43(s, 6H), 3.73(m, 4H), 4.08(m, 4H), 4.20(brs, 2H), 6.25(s, 1 H), 6.90(s, 1 H)

The synthetic route of 236750-65-5 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; VITTAL MALLYA SCIENTIFIC RESEARCH FOUNDATION; WO2007/138612; (2007); A2;; ; Patent; VITTAL MALLYA SCIENTIFIC RESEARCH FOUNDATION; WO2007/138613; (2007); A2;,
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts