Related Products of 79463-77-7, A common heterocyclic compound, 79463-77-7, name is Diphenyl N-cyanocarbonimidate, molecular formula is C14H10N2O2, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
Compound 42 (424 mg, 1.78 mmol) in 2-propanol (40 mL) was treated with adamantane-1-methylamine hydrochloride (23)18 (357 mg, 1.77 mmol) and triethylamine (300 muL, 2.16 mmol) and the homogeneous solution was stirred at room temperature for 18 h. The resulting precipitate was collected by filtration, washed with diethyl ether (10 mL) and dried under vacuum to give 52 as a white solid (275 mg, 50%). Data matched that previously reported.18
The synthetic route of 79463-77-7 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Callis, Timothy B.; Reekie, Tristan A.; O’Brien-Brown, James; Wong, Erick C.N.; Werry, Eryn L.; Elias, Nabiha; Jorgensen, William T.; Tsanaktsidis, John; Rendina, Louis M.; Kassiou, Michael; Tetrahedron; vol. 74; 12; (2018); p. 1207 – 1219;,
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts