Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 3544-25-0, name is 2-(4-Aminophenyl)acetonitrile, This compound has unique chemical properties. The synthetic route is as follows., COA of Formula: C8H8N2
Take carbazole monoaldehyde 0.502g (2mmol)Add about 3 mL of dichloromethane to a 100 mL round bottom flask to dissolve completely.Then, 0.3 g of p-aminophenylacetonitrile and 30 mL of ethanol were added to the flask.1.5 mL of TBAH (tetrabutylammonium hydroxide) was added dropwise as a catalyst.The progress of the reaction was monitored by thin layer chromatography and reacted at 80 C for 12 hours.The reaction mixture was cooled and a small amount of yellow precipitate was precipitated.Dry the organic phase to a yellow solid, dissolve it with a small amount of dichloromethane and pour it into a beaker.Add 100mL of ethanol and stir. A large amount of yellow solid precipitates and is quickly filtered.The solid obtained by suction filtration was washed three times with ethanol.The collected solid was dried and weighed 0.44 g of an orange-red solid with a yield of about 60%.
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 3544-25-0.
Reference:
Patent; Anhui University; Zhu Weiju; Fang Min; Liu Xiaonan; Ge Jialong; Li Cun; Wu Zhenyu; (12 pag.)CN108640867; (2018); A;,
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