1953-99-7, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 1953-99-7, name is 3,4,5,6-Tetrachlorobenzene-1,2-dicarbonitrile belongs to nitriles-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
3,4,5,6-Tetrachlorophthalonitrile (10 g), Potassium carbonate (10 g), Dodecane thiol (10 g) and Tetrahydrofuran (100 ml) were added to a 500 ml flask and reacted at room temperature for 2 hours.After completion of the reaction, the reaction mixture was filtered and vacuum distilled, and then hexane (100 mL) was added thereto for purification and filtration to obtain 4-dodecathio-3,5,6-trichlorophthalonitrile (11 g).
The synthetic route of 3,4,5,6-Tetrachlorobenzene-1,2-dicarbonitrile has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Samsung SD I Co., Ltd.; Park, In Kul; Kim, Hyung Mook; Park, Chae Won; Sin, Myung Yeop; Lee, Young Gi; Jung, Uii Soo; (31 pag.)KR2016/47824; (2016); A;,
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts